Genre:
Baum- und Umwelttechnik
Autor:
Teresa Sherma, Joseph Kowalska
Herausgeber:
Taylor and Francis
Erscheinungsdatum:
22.06.2007
Zusatztext "Within Thin Layer Chromatography in Chiral Separations and Analysis the editors succeeded very well in producing a comprehensive! yet accessible! source of information! having won respected specialists in this field. It provides an excellent overview of the subject both in theoretical and practical aspects." -Dr. W. Schwack! University of Hohenheim! in CAMAG Bibliography Service! April 2008"In 15 chapters of the book! written by 24 authors (many with well recognized achievements in the analysis of chiral compounds)! all important aspects of the separation and analysis of enantiomers by planar chromatography are covered . . . One advantage of this monograph is the extensive literature cited by the authors! and in most chapters the references contain the full titles of the articles cited . . . publication is very timely." - Edward Soczewinski! in Journal of Chromatographic Science! 2008 Informationen zum Autor Kowalska, Teresa; Sherma, Joseph Klappentext Investigation and control of chirality! which is executed almost exclusively using chromatographic techniques! ranks among the most difficult separation tasks. As the first book devoted to this topic! Thin Layer Chromatography in Chiral Separations and Analysis presents updated information on this important field. The first part of this book discusses the problem of chirality in general and the technical possibilities of carrying out enantiomer separations in detail. Addressing significant application areas! the second part of the text provides a comprehensive overview of enantioseparations and densitometric analyses that have been successfully achieved using thin layer chromatography. Zusammenfassung Thin Layer Chromatography in Chiral Separations and Analysis is the first book to focus solely on the theory, capabilities, and applications of TLC for direct and indirect enantioseparations. The first part of the book examines the fundamental principles of chirality and TLC. It describes the necessary materials, laboratory equipment, proced Inhaltsverzeichnis Introduction. Chirality. Commercial Stationary Phases for Enantioseparations. Planar Chromatographic Enantioseparations on Non-commercial CSPs. Planar Chromatographic Enantioseparations on Non-Commercial CCPs. Chiral Modifiers of Mobile Phases. An Overview of the Chiral Separation Mechanisms. Separation of Diastereoisomers by means of TLC. Selected Bottlenecks of Densitometric Detection with Chiral Analytes. Chirality of Pharmaceutical Product Racemates. Chiral Separation of the Selected ß-blockers. Chiral Separation of Aminoacid Enantiomers. Chiral Separation of NSAIDs. Determination of Components in Selected Drug Racemates. Chiral Separations using Marfey's Reagent. ...
Autorentext
Kowalska, Teresa; Sherma, Joseph
Klappentext
Investigation and control of chirality, which is executed almost exclusively using chromatographic techniques, ranks among the most difficult separation tasks. As the first book devoted to this topic, Thin Layer Chromatography in Chiral Separations and Analysis presents updated information on this important field. The first part of this book discusses the problem of chirality in general and the technical possibilities of carrying out enantiomer separations in detail. Addressing significant application areas, the second part of the text provides a comprehensive overview of enantioseparations and densitometric analyses that have been successfully achieved using thin layer chromatography.
Zusammenfassung
Thin Layer Chromatography in Chiral Separations and Analysis is the first book to focus solely on the theory, capabilities, and applications of TLC for direct and indirect enantioseparations. The first part of the book examines the fundamental principles of chirality and TLC. It describes the necessary materials, laboratory equipment, proced
Inhalt
Introduction. Chirality. Commercial Stationary Phases for Enantioseparations. Planar Chromatographic Enantioseparations on Non-commercial CSPs. Planar Chromatographic Enantioseparations on Non-Commercial CCPs. Chiral Modifiers of Mobile Phases. An Overview of the Chiral Separation Mechanisms. Separation of Diastereoisomers by means of TLC. Selected Bottlenecks of Densitometric Detection with Chiral Analytes. Chirality of Pharmaceutical Product Racemates. Chiral Separation of the Selected -blockers. Chiral Separation of Aminoacid Enantiomers. Chiral Separation of NSAIDs. Determination of Components in Selected Drug Racemates. Chiral Separations using Marfey's Reagent.
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